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General workflow - Coggle Diagram
General workflow
Feces test
Dry
Bird, Cow, Deer, Dog, Human, HorseWG, HorseC, HorseMWG, Pig
0.05 g of feces
US for human wet and human dry
IS needed?
Yes, 10 mkg x (9+6+2)
ASE DCM/MeOH 3:2
Wet
Deer, Dog, Human, HorseWG, HorseC, HorseMWG
P&A test
6 BA mixture of 0.1-0.0001 mg/ml, check the linearity of log plot
IS Needed?
No
Solubility test
6 BA mixture dissolved in MeOH, dried up and redissolved in solvents
Water/ ACN (10-60%)
ACN/ MeOH (50-70%)
IS needed?
No
Matrix test
10 mkg of BA added directly to the cell
Filter
Blank
sediments
(wet)
Sand
Blank sediments (dry)
Blank soil (wet)
Blank soil (dry)
For soil and sediments, check 2 methods of ASE
IS needed?
Yes, 10 mkgx10
Fractionation loss test
10 mkg of 6 BA in MeOH placed directly to the column
V1
F1: Tol
F2: MeOH/Tol 2:1
V2
F1: Tol
F2: DCM/MeOH 2:1
Yes, 10 mkg x 3
V3
F1: Tol
F2: Tol/MeOH 1:1
F3: MeOH