L08 Summary

Composite testing

Destructive testing

**very important to quantify material properties and detects defects of material

  • Design Data (can the material withstand the load)
  • Quality control (does it meet criteria, check for defects)
  • Failure analysis (find cause of failure)
  • Repair and Maintainence (check for damage, where is the damage)

defects in component (manufacturing)

defects in component (service)

  • porosity (when stir to fast, bubble will form)
  • fiber misalignment (material properties will become weaker -> it will not able to withstand load that will be applied)
  • crack delamination (thermal stress)
  • wavy fiber (fibers not align)
  • impact
  • debonding (did not put adhesive / not cure at the proper temperature)
  • Bolt hole damage (residual & thermal stresses -> cause crack)
  • moisture ingression (moisture absorb -> can cause corrosion)

** will cause damage

  • costly (materials need to be cut)
  • time consuming (many sample)
  • specimen are selected at random from a large piece to have good indication of result
    must perform according to ISO / ASTM standard

Resin, Fiber and Void Content

  • during manufacturing, high chance that voids will be produced (depends how many % of voids accepted)
  • 2 methods to determine the Resin, Fiber and Void content
  1. Matrix Ignition Loss Method (fiberglass)
  2. Matrix Digestion Method
  • Material inside acid solution > matrix will dissolve > residue is reinforcement > filtered > wash > dry > cool > weigh
  • calculate fiber volume fraction assuming the void content is 0 by using the formula

image

Microscopy

Determine microstructural parameters:

  1. voids
  2. fiber orientation
  3. spatial distribution of fiber
  4. ply count
  5. delamination

Sample preparation is very important before sample can be viewed under microscope:

  1. sectioning
  2. mounting
  3. grinding and polishing

Mechanical Testing

  • Destructive -> require to test sample at a specific shape
  • test develop for metals and plastic usually cannot be used for composites
  • due to the anisotropic nature of composite, large no. of test are usually requires to fully characterized the material
  • different fixtures are used to adapt the machine for different test
  • Short beam shear test > used to bend the sample > allow to measure interlaminar shear strength
  • similar to flexural test
  • difference is that the material is shorter, the span length is also shorter > minimize flexural and maximise shear stress
  • force will be in the middle with 2 support
  • longitudinal waves
  • V-notch beam testing method (in plane shear) -> iosipesco method
  • force will be at both top and bottom (diagonally)

Compression after impact (residual strength) -> drop weight of known mass > impact energy is controlled by the height of the mass

ASTM / ISO guidelines:

  1. Specimen shape and size
  2. Precaution to be taken test set up and apparatus
  3. Specimen conditioning
  4. Acceptable failure mode
  5. Calculation and report

Material property Data:

  • Fiber volume ratio
    -> load bearing properties
    -> higher fiber > strength material properties
    -> help to withstand high load
  • Tensile properties
  • Shear properties
  • Flexural properties
  • Compressive properties

Non Destructive testing

Testing Condition:

  • Machining effects
  • Alignment of specimen
  • Conditioning and environmental test chamber

Acceptable and Unacceptable failure modes


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The main techniques used for composites parts are:

  1. Visual inspection
  2. Tap testing
  3. Ultrasonic
  4. Radiographic
  5. Thermography

**will not cause damage

Visual Inspection

  • damage such as dent, penetration, crack can be observe
  • visual aids: fiberscope, boroscope, magnifying glass, mirrors
  • only surface defects can be detected

Tap Testing

  • damage present when there is a change in sound
  • indicative of an underlying defect
  • automated tap testing cannot detect deep damages / small defects

Ultrasonic

  • ultrasonic wave or energy will absorbed / reflected when there is damage
  • travel through the material (no crack echo)
  • image
  • velocity = distance/time
  • distance of defect = velocity x time
  • air gap between transducer & specimen causes ultrasonic energy to reflect
  • little energy pass through specimen
  • couplant displace the air gap and facilitate the transmission of ultrasonic energy from the transducer into the test specimen

Angle Beam Technique

  • detect any flaws that is covered
  • wedges are attached at various angles to cause refraction
  • wedges are often used by straight beam probes to shield the surface of the transducer from scratches/abrasion.
  • image
  • transverse / shear waves

calibration

performed before ultrasonic testing

Data representation

  • A scan (plot of signal amplitude against time)
  • B scan (transducer is move across the sample to generate cross-sectional view
  • C scan (top view of scanned part)
    -> transducer move systematically

advantages

disadvantages

  • detect deep defects
  • determine size and shape
  • safe method
  • less suitable for large-area inspection
    -> slow scanning and coupling needed
  • not appropriate for thin component scanning
  • required calibration standards
  • thorough preparation needed for interpreting signals

Bond Testing

  • Unlike conventional ultrasonic testing, bond testers uses a dual element probe that contains two elements
  • One element transmits sound waves and the other element receives the waves.
  • As audible sound energy is used, little loss of energy occurs and hence couplant is not needed.
  • The presence of defects will cause changes in the amplitude and/or phase of the received sound waves.

Thermography

  • consists of all procedures used to calculate temperature differences for sections under examination by heat sensing instruments.
  • commonly, heat source is present to heat up the component that is being tested
  • once the part cools down, infrared camera monitor the part
  • can detect debonding, delamination, inclusion and thickness and density variations
  • defect-free areas conduct heat more successfully than areas with defects, showing the amount of heat reflected where any defects are present.
  • can inspect large area quickly
  • couplant are not needed
  • suitable for thin laminates or when defects are near the surface
  • difficult to detect deep defects